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1 H NMR (400 MHz, DMSO- d 6 ) δ 12.31 (s, 1H), 11.13 (s, 1H), 7.88 (d, J = 8.2 Hz, 1H), 7.84–7.76 (m, 1H), 7.64 (d, J = 7.1 Hz, 1H), 7.40 (s, 1H), 6.73 (d, J = 4.9 Hz, 1H), 5.12 (dd, J = 12.8, 5.4 Hz, 1H), 4.41 (d, J = 12.7 Hz, 1H), 4.06 (s, 2H), 3.91 (d, J = 12.9 Hz, 1H), 3.19–3.13 (m, 2H), 3.05 (t, J = 11.8 Hz, 1H), 2.89 (td, J = 13.5, 6.4 Hz, 1H), 2.74 (t, J = 11.2 Hz, 1H), 2.68–2.52 (m, 5H), 2.11–2.02 (m, 1H), 1.92–1.77 (m, 4H), 1.63–1.51 (m, 1H), 1.48–1.37 (m, 1H), 1.18 (s, 9H)