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10.2.1.7 Operational parameters for gas chromatography (a) Packed column Column: Material: Glass Length: 2 m Inner diameter: 2.2 mm Stationary phase: Porapak Q 100-120 mesh Detector: Thermoionic nitrogen detector Temperatures: Column: 120 °C Injector: 220 °C Detector: 300 °C Carrier gas: Helium: 30 ml/min Detector gases: Hydrogen: 3 ml/min Synthetic air: 60 ml/min Injected head-space 50 µl Under these conditions, hydrogen cyanide has a retention time of 1.5 min

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